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FRAC-PAK

Function

A unique new product used to cure severe and total loss of circulation in synthetic, diesel and water muds.

 

General Description

A mixture of inert material and cellulose fiber used to prepare a high solids pill to be squeezed into loss circulation zones. Once in place in a loss zone, the liquid is squeezed out leaving behind a solid plug.

 

Product Benefits

  1. Eliminates need to maintain LCM in total mud system.
  2. Cures lost circulation rather that temporarily reducing losses.
  3. Eliminates risk of side-tracking such as occurs with cementing.
  4. Can be acidized if necessary.

Product Description

  • Color: Off white
  • Form: Fine Powder
  • Specific Gravity: 2.0
  • Bulk Density: 12-15 lbs./cu. ft.
  • pH: 6-8
  • Packaging: 25 lb 3-ply bag w/poly liner

Typical Treatment:
  • Mix 50-100 bbl pill containing 50-100 bl/bbl of material. Mix in water (oil can be used) and add barite to obtain desired density.
  • Squeeze into loss zone and hold pressure for 10-15 minutes.
  • Pull up to safe place for 2 hours and resume operation.

 

Mixing & Spotting Procedure:

1.     Ideally enough slurry should be available to cover all potential loss zones, and 50% excess for squeezing operations. Remember that this is a mechanical set pill and the finished product could be appreciably less than 50% of what you started with.


2.     No special equipment is needed to mix or pump the FRAC-PAK slurries. The slurry can be mixed in a clean uncontaminated mud pit and pumped with rig pumps. It is best to physically monitor the volume of slurry pumped from the mixing tank, then reset the stroke counter to zero to count the strokes to place the slurry. This gives better control and insures the slurry is properly picked up and spotted.
 

3.     It is generally best to begin with 80% of the liquid volume of fluid (as per tables 1,2,or 3).

To the fluid add:
a.  1 – 2 defoamer when using water;
b.  all the FRAC-PAK;
c.  barite;
d.  remainder of the fluid.
When mixing in diesel or oil mud, additional wetting agent is required.  Always pilot test for proper concentration.
When mixing in fresh or salt water, an additional thinner may be required.  Always pilot test for proper concentration.


4.     The slurry should be weighted to the same as the drilling fluid in the hole.

5.     An additional 5 to 20 ppb medium size LCM will often be beneficial depending upon hole conditions. To avoid plugging the drill string, be certain that any additional LCM is smaller than any restrictions in the drill string.

6.     Place the bottom of the drill pipe or bit at depth that will allow the slurry to clear the drill string plus 5 bbls of slurry.


7.     Pump the slurry at 2 bbls per minute until slurry plus 5 bbls clears the drill string.


8.     Pump approximately 20% of slurry into thief zone at 1 bbl/min.


9.     Shut down and observe well. Before beginning the hesitation squeeze, check the annulus. If no fluid can be seen, attempt to fill the backside.


10.  Close the annular BOP and begin pumping the hesitation squeeze down the backside at .25 to .5 bbls/min. in 5 bbls increments or when a pressure of 50 psi is obtained discontinue pumping for 15 minutes. Repeat this procedure until 50 psi can be maintained, and then attempt at progressively higher pressures in 25 psi increments. With this hesitation squeeze method there will be a pressure bleed off each time the pump is stopped. However, with each successive squeeze, the pressure should stabilize at a higher level.


11.  When the maximum holding pressure is obtained, shut down and wait for four hours.


12.  Bleed pressure from annulus slowly, and then circulate any water/oil and remaining FRAC-PAK out of the hole.


13.  Begin staging in the hole slowly monitoring the weight indicator, and checking for bridges. Wash to bottom drilling any FRAC-PAK plug encountered. FRAC-PAK will not set up like cement, so there is no danger of sidetracking the hole.

   Additional FRAC-PAK Suggestions:

  •   Do not contaminate FRAC-PAK slurry with low fluid-loss mud or fluid loss additives.
  •   Do not hurry to build squeeze pressure. Patience and time are necessary to obtain a successful squeeze.
  •   Do not mix a weighted slurry too far in advance of using it. All weighted fluids are subject to barite settling with  time.

Slurry Formulations

 

TABLE I

Formula for preparing one barrel of FRAC-PAK weighted slurry with fresh water, bay water or seawater. A thinner may be required with this formula.

 

Density
FRAC-PAK
Barite
Water

Lb./Gal

Lb.
 Sack
Bbl.
9.0
100
 0
.89
10.0
100
 0.6
.86
11.0
94
 1.2
.82
12.0
84
 1.8
.79
13.0
78
 2.3
.76
14.0
70
 2.9
.72
15.0
62
 3.5
.69
16.0
56
 4.0
.65
17.0
48
 4.6
.62
18.0
44
 5.2
.58
19.0
34
 5.8
.54

 

 

TABLE II

Formula for preparing one barrel of FRAC-PAK weighted slurry with saturated salt water.  A thinner may be required with this formula.

 

 

Density
FRAC-PAK
Barite
Water

Lb./Gal

Lb.
 Sack
Bbl.
10.5
100
 0
.94
11.0
100
 .3
.91
12.0
89
 .9
.88
13.0
83
 1.6
.85
14.0
77
 2.2
.81
15.0
71
 2.8
.77
16.0
65
 3.4
.74
17.0
59
 4.0
.70
18.0
52
 4.6
.66
19.0
46
 5.2
.62
      

 

 

*TABLE III

Formula for preparing one barrel of FRAC-PAK weighted slurry with 7.0 ppg base oil.

 

Density
FRAC-PAK
Barite
Oil

Lb./Gal

Lb.
 Sack
Bbl.
8.0
88
 0.1
0.82
9.0
82
 0.6
.80
10.0
75
 1.1
.78
11.0
70
 1.7
.75
12.0
64
 2.2
.72
13.0
60
 2.8
.69
14.0
54
 3.3
.67
15.0
48
 3.8
.65
16.0
44
 4.4
.62
17.0
38
 4.9
.60
18.0
32
 5.5
.57

 

*A wetting agent is required with this formula.  Pilot test is necessary to determine quantity of wetting agent, to achieve a free flowing slurry.

 

The major key to a successful FRAC-PAK job is placing the slurry at the proper location in the wellbore so the liquid phase can be properly squeezed from the slurry leaving behind the reinforced solid plug.
 

                                                                               

                                            

 

 

 

 

MATERIAL  SAFETY  DATA  SHEET
BOYSENBLUE/CELTEC INTERNATIONAL, INC.

P. O. Box 53648

 Lafayette, LA  70505      



         
I.              MATERIAL IDENTIFICATION

Name:                FRAC-PAK                                                                                CAS Reg. No:               Mixture
Chemical Family:                                                                                                Product Information No:
                                                                                                                (337)  233-1121
This product is in U.S. Commerce, and is listed in the Toxic Substances Control Act (TSCA) Inventory of Chemicals; hence, it may be subject to applicable TSCA provisions and restrictions.

 


II.             HAZARDOUS INGREDIENTS

Ingredients       CAS                             %                                                            OSHA           ACGIH
                                                              Number                   By Wt.                                      PEL                                       TLV        
Calcium Hydroxide                            1305-62-0                    8                                       5 mg/m3                          5 mg/m3
Crystalline silica (Quartz)               14808-60-7                   < 1                                0.1 mg/m3*                   0.1mg/m3
Proprietary**                                       Various                        > 91                                        NE                                  NE
*  Respirable Dust
** The specific chemical identity of this material is being withheld as a trade secret. It will be provided in        accordance with provisions of 29 CFR Part 1910.1200 (i). In the event of a medical emergency, it will be     provided to a treating physician or nurse through utilization of the above Emergency Telephone                  Number.

 

III.            PHYSICAL DATA

Appearance:                         Buff to off-white powder                      Specific Gravity:                    2.1
Odor:                                      Odorless                                              Solubility/water:                    < 9 %
PH:                                    11.5
DOT Class:                           Not regulated
NFPA/HMIS:  Health – 0     Fire – 0  Reactivity – 0        Specific Hazard – 0
Calcium Hydroxide:  CAS No. 1305-62-0; 8% by weight; 5 mg/m3 OSHA PEL; 5 mg/m3 ACGIH TLV

IV.           REACTIVITY DATA                                              

Stable: X                Unstable:
Hazardous Combustion or Decomposition Products: Not Established
Incompatibility (materials to avoid): Fluorine, Oxygen Difluoride, Chlorine, Trifluoride, Hydrofluride Acid.
Hazardous Polymerization:  Will not occur
                                                                                                                                                                                                               
V.            FIRST AID MEASURES

Skin:  Not absorbed by the skin.  May cause dryness.  Use moisture renewing lotions if dryness occurs.
Eye:  May cause irritation or inflammation.  Wash with generous quantities of water.  Consult physician if irritation persists.
Inhalation:  Acute inhalation can cause dryness of the nasal passages and congestion of the upper respiratory tract.  Remove to fresh air.
Ingestion:  Short-term exposure not considered harmful.  Drink generous amounts of water to reduce bulk and drying effects.
               

VI.           FIRE AND EXPLOSION DATA

Flash Point (method used)                                               Not Applicable
Flammable Limits in Air % By volume:                           Lower: Not Applicable    Upper: Not Applicable
Special Fire Fighting Procedures: Evacuate area of all unnecessary personnel. Use NIOSH approved self contained breathing apparatus (SCBA) and other protective equipment and/or garments as conditions warrant.
Extinguishing Media: Water, foam, dry chemical, carbon dioxide.
Unusual Fire & Explosion Hazards:                                Not Applicable
Hazardous Combustion Products:                                  Not Applicable

VII.          HEALTH HAZARDS

OSHA Permissible Exposure Limit:  None Established
AGGIH Threshold Limit Value:          None Established
Effects of Overexposure:                   May cause eye irritation with contact, and may irritate mucus membranes of the nose, throat and upper respiratory tract. Ingestion may cause irritation to the gastrointestinal tract.
Listed as Carcinogen Potential Carcinogen:  No

VIII.         SPILL, LEAK, AND DISPOSAL PROCEDURES

In Case of Spill or Leak: Waste Disposal Method: Flushing and Rinsing
EPA Registry Number:  None
               

IX.           PROTECTIVE INFORMATION

Respiratory Protraction:  Use NIOSH approved respirator for protection against dust.
Ventilation:  Use adequate mechanical ventilation.
Protective Gloves: Rubber or neoprene
Eye Protection:  Safety Goggles or Face Shield
Other Protective Equipment: Synthetic apron

X.            SPECIAL PRECAUTIONS

Precautions to be taken in Handling and Storing:  Caution should be taken with this material so that prolonged of skin contact and contact with eyes does not occur.
Personal Protective Equipment:

 

The above data is based on tests and experience which Boysenblue/Celtec International believes reliable and are supplied for international disclaims any liability for damage or injury which results from the use of the above data and nothing contained therein shall constitute a guarantee, warranty (including freedom from patent liability) by Boysenblue/Celtec International with respect to the data, the product described, or their use for any specific purpose, even if that purpose is known to Boysenblue/Celtec International.



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